2020

(179) S. M. Pugh, P. A. Wright, D. J. Law, N. Thompson and S. E. Ashbrook,

Facile, Room-Temperature 17O Enrichment of Zeolite Frameworks Revealed by Solid-State NMR Spectroscopy,

10. J.Am. Chem. Soc. in press (2020).
    

2019

(178) R. F. Moran, D. McKay, P. C. Tornstrom, A. Aziz, A. Fernandes, R Grau-Crespo and S. E. Ashbrook,

Ensemble-Based Modelling of the NMR Spectra of Solid Solutions: Cation Disorder in Y2(Sn,Ti)2O7,

J. Am. Chem. Soc. 141, 17838-17846 (2019).

(177) C. J. Heard, L. Grajciar, C. M. Rice, S. M. Pugh, P. Nachtigall, S. E. Ashbrook and R. E. Morris,

Fast Room Temperature Lability of Aluminosilicate Zeolites,

Nature Commun. 10, 4690-4697 (2019).

(176) D. M. Dawson, C. E. F. Sansome, L. N. McHugh, M. J. McPherson, L. J. McCormick, R. E. Morris and S. E. Ashbrook,

13C pNMR of “Crumple Zone” Cu(II) Isophthalate Metal-Organic Frameworks,

Solid State Nucl. Magn. Reson. 101, 44-50 (2019).

(175) Z. Ke, L. E. Jamieson, D. M. Dawson, S. E. Ashbrook and M. Bühl,

NMR Chemical Shifts of Urea Loaded Copper Benzoate. A Joint Solid-State NMR and DFT Study,

Solid State Nucl. Magn. Reson. 101, 31-37 (2019).

(174) C. Kouvatas, N. Kanwal, J. Trebosc, C. Roiland, L. Delevoye, S. E. Ashbrook, E. Le Fur and L. Le Polles,

Rationalization of Solid-State NMR Multi-Pulse Decoupling Strategies: Coupling of Spin I = ½ and Half-Integer Quadrupolar Nuclei,

J. Magn. Reson. 303, 48-56 (2019).

(173) N. Kanwal, H. Colaux, D. M. Dawson, Y. Nishiyama and S. E. Ashbrook,

Sensitivity Improvement in 5QMAS NMR Experiments Using FAM-N Pulses,

Solid State NMR 100, 1-10 (2019).

(172) S. E. Henkelis, M. Mazur, C. M. Rice, P. S. Wheatley, S. E. Ashbrook and R. E. Morris,

Kinetics and Mechanism of the Hydrolysis and Rearrangement Processes Within the Assembly-Disassembly-Organization-Reassembly Synthesis of Zeolites,

J. Am. Chem. Soc. 141, 4453-4459 (2019).

(171) R. R. Prasad, S. Seidner, D. Cordes, M. M. Lozinska, D. M. Dawson, M. J. Thompson, T. Duren, K. K. Chakarova, M. Y. Mihaylov, K. I. Hadjiivanov, F. Hoffman, A. M. Z. Slawin, S. E. Ashbrook, M. L. Clarke and P. A. Wright,

STA-27, A porous Lewis Acidic Scandium MOF with an Unexpected Topology Type Prepared with Tetracarboxyphenylpyrazine,

J Mater. Chem. A 7, 5685-5701 (2019).

(170) D. McKay, R. F. Moran. D. M. Dawson, J. M. Griffin, S. Sturniolo, C. J. Pickard, A. J. Berry and S. E. Ashbrook,

A Picture of Disorder in Hydrous Wadsleyite – Under the Combined Microscope of Solid-State NMR Spectroscopy and Ab Initio Random Structure Searching,

J. Am. Chem. Soc. 141, 3024-3036 (2019).

(169) S. E. Henkelis, M. Mazur, C. M. Rice, G. P. M. Bignami, P. S. Wheatley, S. E. Ashbrook, J. Cejka, and R. E. Morris,

A Procedure for Identifying Possible Products in the Assembly-Disassembly-Organisation-Reassembly (ADOR) Synthesis of Zeolites,

Nature Protocols, 14, 781-794 (2019).

(168) B. Monserrat, S. E. Ashbrook and C. J. Pickard,

Nuclear Magnetic Resonance Spectroscopy as a Dynamical Structural Probe of High Pressure Hydrogen,

Phys. Rev. Lett. 122, 135501 (2019).

(167) J. Ihli, J. N. Clark, N. Kanwal, Y.-Y. Kim, M. Holden, R. J. Harder, C. C. Tang, S. E. Ashbrook, I. K. Robinson and F. C. Meldrum,

Visualization of the Effect of Additives on the Nanostructures of Individual Bio-Inspired Calcite Crystals,

Chem. Sci. 10, 1176-1185 (2019).

2018

(166) D. M. Dawson, R. F. Moran, S. Sneddon and S. E. Ashbrook,

Is the 31P Chemical Shift Anisotropy of Aluminophosphates a Useful Parameter for NMR Crystallography?,

Magn. Reson. Chem. 57, 176-190 (2018).

(165) D. S. Cook, G. J. Clarkson, D. M. Dawson, S. E. Ashbrook, J. M. Fisher, D. Thompsett, D. M. Pickup, A. V. Chadwick and R. I. Walton,

Alkaline-Earth Rhodium Hydroxides: Synthesis, Structures and Thermal Decomposition to Complex Oxides,

Inorg. Chem. 57, 11217-11224 (2018).

(164) R. Liu, E. Morris, X. Cheng, E. Amigues, K. Lau, B. Kim, Y. Liu, Z. Ke, S. E. Ashbrook, M. Bühl and G. Dawson,

SERS of Trititanate Nanotubes: Selective Enhancement of Catechol Compounds,

Chem. Select 3, 8338-8343 (2018).

(163) H. Kunicki, T. W. Chamberlain, G. J. Clarkson, R. J. Kashtiban, J. E. Hooper, D. M. Dawson, S. E. Ashbrook and R. I. Walton,

An Expanded MIL-53-Type Coordination Polymer with a Reactive Pendant Ligand,

CrystEngComm. 20, 4355-4358 (2018).

(162) S. E. Ashbrook and P. Hodgkinson,

Perspective: Current Advances in Solid-State NMR Spectroscopy,

J. Chem. Phys. 149, 040901 (2018).

(161) R. R. Prasad, D. M. Dawson, P. A. Cox, S. E. Ashbrook, P. A. Wright and M. L. Clarke,

A Bifunctional MOF containing Metal-Phosphine and Lewis Acidic Active Sites,

CrystEngComm. 24, 15309-15318 (2018).

(160) L. N. McHugh, M. J. McPherson, L. J. McCormick, S. A. Morris, S. J. Teat, D. McKay, D. M. Dawson, C. E. F. Sansome, S. E. Ashbrook, C. A. Stone, M. W. Smith and R. E. Morris,

Hydrolytic Stability in Hemilabile Metal-Organic Frameworks,

Nature Chem. 10, 1096-1102 (2018).

(159) J. Sánchez-Laínez, B. Zornoza, A. F. Orsi, M. M. Łozińska, D. M. Dawson. S. E. Ashbrook, S. M. Francis, P. A. Wright, V. Benoit, P. L. Llewellyn, C. Téllez and J. Coronas,

Synthesis of ZIF-93/11 Hybrid Nanoparticles via Post-synthetic Modification of ZIF-93 and their Use for H2/CO2 Separation,

Chem. Eur. J. 24, 11211-11219 (2018).

(158) P. Sanz Camacho, M. W. Stanford, D.McKay, D. M. Dawson, K. S. Athukorala Arachchige, D. B. Cordes, A. M. Z. Slawin, J. D. Woollins and S. E. Ashbrook,

Polymorphism, Weak Interactions and Phase Transitions in Chalcogen-Phosphorus Heterocycles,

Chem. Eur. J. 24, 11067-11081 (2018).

(157) A. Fernandes, R. F. Moran, S. Sneddon, D. M. Dawson, D. McKay, G. P. M. Bignami, F. Blanc, K. R. Whittle and S. E. Ashbrook,

17O Solid-State NMR Spectroscopy of A2B2O7 Oxides: Quantitative Isotopic Enrichment and Spectral Acquisition?,

RSC Advances, 8, 7089-7101 (2018).

(156) A. Bumstead, D. Cordes, D. Dawson, K. Chakarova. M. Mihaylov, C. Hobday, T. Duren, K. Hadjivanov, A. Slawin, S. E. Ashbrook and P. A. Wright,

Modulator-Controlled Synthesis of Microporous STA-26, an Interpenetrated 8,3-Connected Zirconium MOF with the the-i Topology, and its Reversible Lattice Shift,

Chem. Eur. J. 24, 1-13 (2018).

(155) S. E. Ashbrook, J. M. Griffin and K. E. Johnston,

Recent Advances in Solid-State NMR Spectroscopy,

Ann. Rev. Anal. Chem. 11, 485-508 (2018).

(154) G. P. M. Bignami, Z. H. Davis, D. M. Dawson, S. A. Morris, S. E. Russell, D. McKay, R. E. Parke, D. Iuga, R. E. Morris and S. E. Ashbrook,

Cost-Effective 17O Enrichment and NMR Spectroscopy of Mixed-Metal Terephthalate Metal-Organic Frameworks,

Chem. Sci. 9, 850-859 (2018).

(153) M. Mazur, A. M. Arévalo-López, P. S. Wheatley, G. P. M. Bignami, S. E. Ashbrook, A. Morales-García, P. Nachtigall, J. P. Attfield, J. Čejka, R. E. Morris,

Pressure-Induced Chemistry for the 2D to 3D Transformation of Zeolites,

10. J.Mater. Chem A 6, 5255-5259 (2018).
    

2017

(152) D. M. Dawson, V. R. Seymour and S. E. Ashbrook,

The Effects of Extraframework Species on the Structure-Based Prediction of 31P Isotropic Chemical Shifts of Aluminophosphates,

J. Phys. Chem. C 121, 28065-28076 (2017).

(151) L. K. Broom, G. J. Clarkson, N. Guillou, J. E. Hooper, D. M. Dawson, C. C. Tang, S. E. Ashbrook and R. I. Walton,

A Gel Aging Effect in the Synthesis of Open-Framework Gallium Phosphates: Structure Solution and Solid-State NMR of a Large-Pore, Open-Framework Material,

Dalton Trans. 46, 16895-16904 (2017).

(150) A. G. M. Rankin, P. B. Webb, D. M. Dawson, J. Viger-Gravel, B. J. Walder, L. Emsley and S. E. Ashbrook,

Determining the Surface Structure of Silicated Alumina Catalysts via Isotopic Enrichment and Dynamic Nuclear Polarization Surface-Enhanced NMR Spectroscopy,

J. Phys. Chem. C 121, 22977-22984 (2017).

(149) S. Sneddon, J. Kahr, A. F. Orsi, D. J. Price, P. A. Wright and S. E. Ashbrook,

Investigation of Zeolitic Imidazolate Frameworks using 13C and 15N Solid-State NMR Spectroscopy,

Solid State NMR 87, 54-64 (2017).

(148) D. M. Dawson, Z. Ke, F. M. Mack, R. A. Doyle, G. P. M. Bignami, I. A. Smellie, M. Buhl and S. E. Ashbrook,

Calculation and Experimental Measurement of Paramagnetic NMR Parameters of Phenolic Oximate Cu(II) Complexes,

Chem. Commun. 55 10512 (2017).

(147) D. M. Dawson, R. F. Moran and S. E. Ashbrook,

A Computational Investigation of the Empirical Relationships between the Crystal Structure and 29Si Isotropic Chemical Shift in Silica Zeolites,

J. Phys. Chem. C 121, 15198-15210 (2017).

(146) E. Hupf, Truong G. Do, A. Nordheider, M. Wehrhahn, P. Sanz Camacho, S. E. Ashbrook, E. Lork, A. M. Z. Slawin, S. Mebs, J. D. Woollins and J. Beckmann,

Selective Oxidation and Functionalization of 6-Diphenylphosphinoacenaphthyl-5-tellurenyl Species 6-Ph2P-Ace-5-TeX (X = Mes, Cl, O3SCF3). Various Types of P-ETe(II,IV) Bonding Situations (E = O, S, Se),

Organometallics 36, 1566-1579 (2017).

(145) G. P. M. Bignami, D. M. Dawson, V. R. Seymour, P. S. Wheatley, R. E. Morris and S. E. Ashbrook,

Synthesis, Isotopic Enrichment and Solid-State NMR Characterization of Zeolites Derived from the Assembly, Disassembly, Organisation, Reassembly Process,

J. Am. Chem. Soc. 139, 5140-5148 (2017).

(144) R. Giovine, C. Volkringer, S. E. Ashbrook, D. M. McKay, J. Trébosc, T. Loiseau, J.-P. Amoureux, O. Lafon and F. Pourpoint,

Solid-state NMR Proves the Presence of Penta-Coordinated Sc Site in MIL-100(Sc),

Chem. Eur. J., in press.

(143) S. A. Morris, G. P. M. Bignami, Y. Tian, M. Navarro, D. S. Firth, J. Cejka, P. S. Wheatley, D. M. Dawson, W. A. Slawinski, D. S. Wragg, R. E. Morris and S. E. Ashbrook,

In situ solid-state NMR and XRD studies of the ADOR process and the intriguing structure of zeolite IPC-6,

Nature Chem. 9, 1012-1018 (2017).

(142) A. Orsi, D. Price, J. Kahr, R. Pillai, S. Sneddon, S. Cao, V. Benoit, M. Loskinska, D. Cordes, A. M. Z. Slawin, P. Llewellyn, I. Casey, S. E. Ashbrook, G. Maurin and P. A. Wright,

Porous Zinc and Cobalt 2-Nitroimidazolates with a Topology Type Related to Tridymite and a Layered Cobalt 2-Nitroimidazolate Polymorph,

CrystEngComm 19, 1377-1388 (2017).

(141) D. M. Dawson, J. M. Griffin, V. R. Seymour, P. S. Wheatley, S. E. Ashbrook, M. Amri, R. I. Walton, N. Guillou, T. Kurkiewicz and S. Wimperis,

A Multinuclear NMR Study of Six Forms of AlPO-34: Structure and Motional Broadening,

J. Phys. Chem. C 121, 1781-1793 (2017).

(140) D. M. Dawson, R. I. Walton, S. Wimperis and S. E. Ashbrook,

The Ambient Hydration of the Aluminophosphate JDF-2 to AlPO-53(A): Insights from NMR Crystallography,

Acta. Cryst. C73, 191-201 (2017)

(139) H. Colaux, D. M. Dawson and S. E. Ashbrook,

Investigating FAM-N Pulses for Signal Enhancement in MQMAS NMR of Quadrupolar Nuclei,

Solid State NMR 84, 89-102 (2017).

11. (11)R. F. Moran, D. M. Dawson and S. E. Ashbrook,
    

Exploiting NMR Spectroscopy for the Study of Disorder in Solids,

Int. Rev. Phys. Chem. 36, 39-115 (2017).

(137) M. Musa, D. M. Dawson, S. E. Ashbrook and R. E. Morris,

onothermal Synthesis and Characterization of CoAPO-34 Molecular Sieve,

Micro. Meso Mater. 239, 336-341 (2017).

2016

(136) D. Rota Martir, G. J. Hedley, D. B. Cordes, A. M. Z. Slawin, D. Escudero, D. Jacquemin, T. Kosikova, D. Philp, D. M. Dawson, S. E. Ashbrook, I. D. W. Samuel and E. Zysman-Colman,

Exploring the Self-Assembly and Energy Transfer of Dynamic Supramolecular Iridium-Porphyrin Systems,

Dalton Trans. 45, 17195-17205 (2016).

(135) A. Fernandes, D. McKay, S. Sneddon, D. M. Dawson, S. Lawson, R. Veazey, K. R. Whittle and S. E. Ashbrook,

Phase Composition and Disorder in La2(Sn,Ti)2O7 Ceramics: New Insights from NMR Crystallography,

J. Phys. Chem. C, 120, 20288-20296 (2016).

(134) R. Kather, E. Rychagova, P. Sanz Camacho, S. E. Ashbrook, J. D. Woollins, L. Robben, E. Lork, S. Ketkov and J. Beckmann,

Increasing the Brønsted Acidity of Ph2PO2H by the Lewis Acid B(C6F5)3. Formation of an Eight-Membered Boraphosphinate Ring [Ph2POB(C6F5)2O]2,

Chem. Commun. 52, 10992-10995 (2016).

(133) M. Bühl*, S. E. Ashbrook*, D. M. Dawson, R. A. Doyle, P. Hrobarik, M. Kaupp and I. A. Smellie,

Paramagnetic NMR of Phenolic Oxime Copper Complexes - a Joint Experimental and Density Functional Study,

Chem. Eur. J., 22, 15328-15339 (2016).

(132) P. Sanz Camacho, D. McKay, D. M. Dawson, C. Kirst, J. R. Yates, T. F. G. Green, D. B. Cordes, A. M. Z. Slawin, J. D. Woollins and S. E. Ashbrook,

Unusual Homonuclear Intermolecular “Through-Space” J Couplings in Organochalcogen Systems,

Inorganic Chemistry, 55, 10881-10887 (2016).

Editor’s choice

(131) S. E. Ashbrook and D. McKay,

Combining Solid-State NMR Spectroscopy with First-Principles Calculations – A Guide to NMR Crystallography,

Chem. Commun. 52, 7186-7204 (2016).

(130) R. F. Moran, D. McKay, C. J. Pickard, A. J. Berry, J. M. Griffin and S. E. Ashbrook,

Hunting for Hydrogen: Random Structure Searching and Prediction of NMR Parameters of Hydrous Wadsleyite,

Phys. Chem. Chem. Phys. 18, 10173-10181 (2016).

(129) S. E. Ashbrook and D. M. Dawson,

NMR Spectroscopy of Minerals and Allied Materials,

RSC Specialist Periodical Reports Nuclear Magnetic Resonance, 45, 1-52 (2016).

2015

(128) L. S. Konstntinova, I. E. Bobkova, Y. V. Nelubina, E. A. Chulanova, I. G. Irtegova, N. V. Vasilieva, P. S. Camacho, S. E. Ashbrook. G. Hua, A. M. Z. Slawin, J. D. Woollins, A. V. Zibarev and O. A. Ratkin,

[1,2,5]Selenadiazolo[3,4-b]pyrazines: Synthesis from 3,4-Diamino-1,2,5- selenadiazole and Generation of Persistent Radical Anions,

Eur. J. Org. Chem. 25, 5585-5593 (2015).

(127) P. Sanz Camacho, K. S. Athukorala Arachchige, A. M. Z. Slawin, T. F. G. Green, J. R. Yates, D. M. Dawson, J. D. Woollins and S. E. Ashbrook,

Unusual Intermolecular Through-Space J Couplings in P–Se Heterocycles,

J. Am. Chem. Soc. 137, 6172-6175 (2015).

(126) A D. Burrows, L C. Fisher, T. J. Mays, S. P. Rigby, S. E. Ashbrook and D. M. Dawson,

Post-Synthetic Modification of Zinc Metal-Organic Frameworks Through Palladium-Catalysed Carbon-Carbon Bond Formation,

J. Organomet. Chem. 792, 134-138 (2015).

(125) S. E. Ashbrook, M. R. Mitchell, S. Sneddon, R. F. Moran, M. de los Reyes, G. R. Lumpkin and K. R. Whittle,

New Insights into Phase Distribution, Phase Composition and Disorder in Y2(Zr,Sn)2O7 Ceramics from NMR Spectroscopy,

Phys. Chem. Chem. Phys. 17, 9049-9059 (2015).

(124) J. Cepeda,* S. Pérez-Yáñez, B, Garikoitz, O. Luque, P Wright, S. Sneddon and S. E. Ashbrook,

Exploiting Synthetic Conditions to Promote Structural Diversity within the Scandium(III) / Pyrimidine-4,6-dicarboxylate System,

Cryst. Growth Des. 15, 2352-2363 (2015).

(123) L. S. Kostantinova, E. A Knyazeva, A. A. Nefydov, P. S. Camacho, S. E. Ashbrook, J. D. Woollins, A. V. Zibarev and O. A. Ratkin,

Direct Synthesis of Fused 1,2,5-selenadiazoles from 1,2,5-thiadiazoles,

Tet. Lett. 56, 1107-1110 (2015).

(122) J. D. Woollins, A. Nordheider, E. Hupf, B. Chalmers, F. R. Knight, M. Buehl, S. Mebs, L. Checinska, E. Lork, Enno; P. Sanz Camacho, S. E. Ashbrook, K. A. Arachchige, D. Cordes, A. M. Z. Slawin and J. Beckmann,

Peri-Substituted Phosphorus-Tellurium Systems – an Experimental and Theoretical Investigation of the P∙∙∙Te Through-Space Interaction,

Inorg. Chem. 54, 2435-2446 (2015).

(121) F. R. Knight, L. M. Diamond, K. S. Athukorala Arachchige, P. Sanz Camacho, R. A. M. Randall, S. E. Ashbrook, M. Bühl, A. M. Z. Slawin and J. D. Woollins,

Conformational Dependence of Through-Space Tellurium-Tellurium Spin-Spin Coupling in Peri-Substituted Bis(Tellurides),

Chem. Eur. J. 21, 3613-3627 (2015).

2014

(120) A. C. McKinlay, P. K. Allan, C. L. Renouf, M. J. Duncan, S. J. Warrender, D. M. Dawson, S. E. Ashbrook, B. Gil, B. Marszalek, T. Duren, J. J. Williams, C. Charrier, D. Mercer, S. J. Teat and R. E. Morris,

Multirate Delivery of Multiple Theapeutic Agents from Metal-Organic Frameworks,

APL Materials 2, 2124108 (2014).

(119) D. Carnevale, S. E. Ashbrook and G. Bodenhausen,

Solid-state NMR Measurements and DFT Calculations of the Magnetic Shielding Tensors of Protons of Water Trapped in Barium Chlorate Monohydrate,

RSC Advances 4, 56248-56258 (2014).

(118) V. R. Seymour, E. C. V. Eschenroeder, P. A. Wright and S. E. Ashbrook,

An NMR Crystallographic Approach to Monitoring Cation Substitution in the Aluminophosphate STA-2,

Solid State NMR in press.

(117) S. E. Ashbrook and S. Sneddon,

New Methods and Applications in Solid-State NMR Spectroscopy of Quadrupolar Nuclei,

J. Am. Chem. Soc. 136, 15440-15456 (2014).

(116) L. Mitchell, P. Williamson, B. Ehrlichova, V. R. Seymour, S. E. Ashbrook, N. Acerbi, M. Daturi, L. Daniels, R. I. Walton, M. L. Clarke and P. A. Wright,

Mixed-Metal MIL-100(Sc,M) (M=Al, Cr, Fe) for Lewis Acid Catalysis and Tandem C-C Bond Formation and Alcohol Oxidation,

Chem. Eur. J. 51, 17185-17191 (2014).

(115) P. S. Wheatley, P. Chlubna-Eliasova, H. Greer, W. Zhou, V. R. Seymour, D. M. Dawson, S. E. Ashbrook, A. B. Pinar, L. B. McCusker, M. Opanasenko, J. Cejka and R. E. Morris,

Zeolites with Continuously Tuneable Porosity,

Angew. Chemie 126, 1-6 (2014).

(114) D. M. Dawson and  S. E. Ashbrook,

Investigating Relationships between the Crystal Structure and 31P Isotropic Chemical Shifts in Calcined Aluminophosphates,

J. Phys. Chem. C 118, 23285-23296 (2014).

(113) S. Valera, J. E. Taylor, D. S. B. Daniels, D. M. Dawson, K. S. Athukorala Arachchige, S. E. Ashbrook, A. M. Z. Slawin and B. E. Bode,

A Practical, Modular Approach to Multi-spin Systems for Pulsed Electron Paramagnetic Resonance,

J.Org. Chem. 79, 8313-8323 (2014).

(112) H. Colaux, D. M. Dawson and S. E. Ashbrook,

Efficient Amplitude-Modulated Pulses for Triple- to Single-Quantum Coherence Conversion in MQMAS NMR,

J. Phys. Chem. A 118, 6018-6025 (2014).

(111) H. Y. Playford, A. C. Hannon, M. G. Tucker, D. M. Dawson, S. E. Ashbrook, R. J. Kastiban, J. Sloan and R. I. Walton,

Characterisation of Structural Disorder in γ-Ga2O3,

J. Phys. Chem. C 118, 16188-16198 (2014).

(110) K. S. Athukorala Arachchige, P. Sanz Camacho, M. J. Ray, B. A. Chalmers, F. R. Knight, S. E. Ashbrook, M. Bühl, P. Kilian, A. M. Z. Slawin and J. D. Woollins,

Sterically Crowded Tin-Phosphines, Stabilized by Weak Intramolecular Donor-Acceptor Interactions,

Organometallics 33, 2424-2433 (2014).

(109) S. E. Ashbrook, D. M. Dawson and V. R. Seymour,

Recent Developments in Solid-State NMR Spectroscopy of Microporous Materials,

Phys. Chem. Chem. Phys. 16, 8223-8242 (2014).

(108) M. W. Stanford, F. R. Knight, K. S. Athukorala Arachige, P. Sanz Camacho, S. E. Ashbrook, M. Buhl, A. M. Z. Slawin and J. D. Woollins,

Probing Interactions Through Space using Spin-Spin Coupling,

Dalton Trans. 43, 6548-6560 (2014).

(107) S. Sneddon, D. M. Dawson, C. J. Pickard and S. E. Ashbrook,

Calculating NMR Parameters in Aluminophosphates: Evaluation of Dispersion Correction Schemes,

Phys. Chem. Chem. Phys. 16, 2660-2673 (2014).

2013

(106) M. Harunsani, D. Woodward, M. D. Peel, S. E. Ashbrook and R. I. Walton,

Investigation of the Hydrothermal Crystallisation of the Perovskite Solid Solution NaCe1–xLaxTi2O6 and its Defect Chemistry,

10. J.Solid-State Chem. 207, 117-125 (2013).
    

(105) P. Lightfoot, S. E. Ashbrook and M. Peel,

Unusual Phase Behaviour in the Piezooelectric Perovskite System, LixNa1–xNbO3,

Inorg. Chem. 52, 8872-8880 (2013).

(104) V. R. Seymour, E. C. V. Eschenroeder, M. Castro, P. A. Wright and S. E. Ashbrook,

Application of NMR Crystallography to the Determination of the Mechanism of Charge-Balancing in Organocation-Templated AlPO STA-2,

Cryst.Eng.Comm. 15, 8668-8679 (2013). Special Edition on NMR Crystallography.

Highlighted on inside front cover

(103) V. Haquin, M. Etienne, C. Daiguebonne, S. Freslon, G. Calvez, K. Bernot, L. Le Pollès, S. E. Ashbrook, M. R. Mitchell, J.-C. Bünzli, S. V. Eliseeva, O. Guillou,

Color and Brightness Tuning in Heteronuclear Lanthanide Terephthalate Coordination Polymers,

Eur. J. Inorg. Chem. 3464-3476 (2013).

(102) W. J. Roth, P. Nachtigall, R. E. Morris, P. S. Wheatley, V. R. Seymour, S. E. Ashbrook, P. Chlubná, L. Grajciar, M. Položij, A. Zukal, O. Shvets, and J. Cejka,

A Family of Complex Zeolites with Controlled Pore Size Prepared through a ‘Top Down’ Method,

Nature Chemistry 5, 628-633 (2013).

(101) J. M. Griffin and S. E. Ashbrook,

Solid-State NMR of High-Pressure Silicates in the Earth’s Mantle,

Ann. Rep. NMR Spectrosc. 79, 241-332 (2013).

(100) S. E. Ashbrook and D. M. Dawson,

Exploiting Periodic First-Principles Calculations in NMR Spectroscopy of Disordered Materials,

Acc. Chem. Res. 46, 1964-1974 (2013). Special Edition on Advances in Solid-State NMR

(99) K. E. Johnston, M. R. Mitchell, F. Blanc, P. Lightfoot and S. E. Ashbrook,

A Structural Study of La1−xYxScO3, Combining Neutron Diffraction, Solid-State NMR and First-Principles DFT Calculations,

J. Phys. Chem. C 117, 2252-2265 (2013).

(98) J. M. Griffin, A. J. Berry, D. J. Frost, S. Wimperis and S. E. Ashbrook,

Structural Chemistry of Water in the Inner-Earth: A Solid-State NMR Study of Hydrous Wadsleyite,

Chem. Sci. 4, 1523-1538 (2013).

(97) M. de los Reyes, K. R. Whittle, S. E. Ashbrook, Martin R. Mitchell, Z. Zhang, L.-Y. Jang and G. R. Lumpkin,

The Pyrochlore to Defect Fluorite Phase Transition in Y2Sn2–xZrxO7,

RSC Advances, 3, 5090-5099 (2013).

(96) D. M. Dawson, L. E. Jamieson, M. I. H. Mohideen, A. C. McKinlay, I. A. Smellie, R. Cadou, N. S. Keddie, R. E. Morris, S. E. Ashbrook,

High-Resolution Solid-State 13C NMR Spectroscopy of the Paramagnetic Metal–Organic Frameworks, STAM-1 and HKUST-1,

Phys. Chem. Chem. Phys. 15, 919-929 (2013).

2012

(95) F. R. Knight, R. A. M. Randall, K. S. A. Arachchuge, L. Wakefield, J. M. Griffin, S. E. Ashbrook, M. Buhl, A. M. Z. Slawin and J. D. Woollins,

Non-Covalent Interactions in Peri-Substituted Chalconium Naphthalene and Acenaphthene Salts: a Combined Experimental, Crystallographic, Solid-State NMR and Computational Study,

Inorg. Chem. 51, 11087-11097 (2012).

(94) C. Bonhomme, C. Gervais, F. Babonneau, C. Coelho, F. Pourpoint, T. Azaïs, S. E. Ashbrook, J. M. Griffin, J. R. Yates, F. Mauri, and C. J. Pickard,

First-Principles Calculation of NMR Parameters Using the GIPAW (Gauge Including Projector Augmented Wave) Method: a Chemistry Point of View,

Chem. Rev. 112, 5733-5779 (2012).

(93) M. Amri, S. E. Ashbrook, D. M. Dawson, J. M. Griffin, R. I. Walton and S. Wimperis,

A Multinuclear Solid-State NMR Study of Templated and Calcined Chabazite-Type GaPO-34,

J. Phys. Chem. C 116, 15048 (2012).

(92) E. Davies, M. J. Duer, S. E. Ashbrook and J. M. Griffin,

Applications of NMR Crystallography to Problems in Biomineralisation: A Refinement of the Crystal Structure and 31P Solid-State NMR Spectral Assignment of Octacalcium Phosphate,

J. Am. Chem. Soc. 134, 12508-12515 (2012).

(91) M. D. Peel, S. P. Thompson, A. Doud-Aladine, S. E. Ashbrook and P.  Lightfoot,

New Twists on the Perovskite Theme: Crystal Structures of the Elusive Phases R and S of NaNbO3,

Inorg. Chem. 51, 6786-6889 (2012).

(90) J. M. Griffin, L. Clark, V. R. Seymour, D. W. Aldous, D. M. Dawson, D. Iuga, R. E. Morris and S. E. Ashbrook,

Ionothermal synthetic routes to efficient 17O enrichment and solid-state NMR of oxide-based materials using microliter quantities of labelled water,

Chem. Sci. 3, 2293-2300 (2012).

(89) M. R. Mitchell, D. Carnevale, R. Orr, K. R. Whittle and S. E. Ashbrook,

Exploiting the Chemical Shielding Anisotropy to Probe Structure and Disorder in Ceramics: 89Y MAS NMR and First-Principles Calculations,

J. Phys. Chem. C. 116, 4273-4286 (2012).

(88) M. T. Wharmby, G. Pearce, J. P. Mowat, J. M. Griffin, S. E. Ashbrook, P. A. Wright, L. H. Schilling, N. Stock, S. Chavin, S. Bordiga, E. Garcia, G. Pirngruber, M. Vreeke and L. Gora,

Synthesis and Crystal Chemistry of the STA-12 Family of N-N’-piperazinebis(methylenephosphonates) and Applications of STA-12(Ni) in the Separation of Gases,

Micro. and Meso. Mater. 157, 3-17 (2012).

(87) J. P. S. Mowat, V. R. Seymour, J. M. Griffin, S. P. Thompson, A. M. Z. Slawin, D. Fairen-Jimenez, T. Duren, S. E. Ashbrook and P. A. Wright,

A Novel Structural Form of MIL-53 Observed for the Scandium Analogue and its Response to Temperature variation and CO2 Adsorption,

Dalton Trans. 4, 3937-3941 (2012).

2011

(86) J. P. S. Mowat, S. R. Miller, J. M. Griffin, V. R. Seymour, S. E. Ashbrook, S. P. Thompson, D. Fairen-Jimenez, A.-M. Banu, T. Duren and P. A. Wright,

Structural Chemistry, Monoclinic-to-Orthorhombic Phase Transition and CO2 Adsorption Behaviour of the Small Pore Scandium Terephthalate, Sc2(O2CC6H4CO2)3 and its Nitro- and Amino-Functionalised Derivatives,

Inorg. Chem. 50, 10844-10858 (2011).

(85) J. M. Griffin, A. J. Berry and S. E. Ashbrook,

Observation of “Hidden” Magnesium: First-Principles Calculations and 25Mg Solid-State NMR of Enstatite,

Solid State Nucl. Magn. Reson. 40, 91-99 (2011).

(84) J. M. Griffin, F. Knight, G. Hua, J. Ferrara, S. Hogan, J. D. Woollins and S. E. Ashbrook,

77Se Solid-State NMR of Inorganic and Organoselenium Systems: A Combined Experimental and Computational Study,

J. Phys. Chem C. 115, 10859-10872 (2011).

(83) A. L. Picone, S. J. Warrender, A. M. Z. Slawin, D. M. Dawson, S. E. Ashbrook,  P. A. Wright, S. P. Thompson, L. Gaberova, P. L. Lewellyn, B. Moulin, A. Vimont, M. Daturi, M. B. Park, S. K. Sung, I. S. Nam, and S. B. Hong.

A Co-templating Route to the Synthesis of Cu SAPO STA-7, an Active Catalyst for the Selective Catalytic Reduction of NO Microporous and Mesoporous Materials,

Micro. Meso. Mater. 146, 36-47 (2011).

(82) K. E. Johnston, J. M. Griffin, R. I. Walton, D. M. Dawson, P. Lightfoot and S. E. Ashbrook,

93Nb NMR and DFT Investigation of the Polymorphs of NaNbO3,

Phys. Chem. Chem. Phys. 13, 7565-7576 (2011).

(81) G. Hua, J. M. Griffin, S. E. Ashbrook, A. M. Z. Slawin and J. D. Woollins,

Octaselenocycoldodecane,

Angew. Chemie 123, 4209  (2011).

(80) M. I. H. Mohideen, B. Xiao, P. S. Wheatley, Y. Li, A. M. Z. Slawin, D. W. Aldous, N. F. Cessford, T. Duren, X. Zhao, R. Gill, K. M. Thomas, J. M. Griffin, S. E. Ashbrook and R. E. Morris,

Protecting Group and Pore-Discriminating Adsorption Properties of a Hydrophilic-Hydrophobic Metal-Organic Framework,

Nature Chem. 3, 304-310 (2011).

(79) N. S. Barrow, J. R. Yates, S. A. Feller, D. Holland, S. E. Ashbrook, P. Hodgkinson and S. P. Brown,

Towards Homonucelar Solid-State NMR Correlation Experiments for Half-Integer Quadrupolar Nuclei: Experimental and Simulated 11B MAS Spin-echo Dephasing and Calculated 2JBB Coupling Constants for Lithium Diborate,

Phys. Chem. Chem. Phys. 13, 5778-5789 (2011).

(78) J. P. S. Mowat, S. R. Miller, A. M. Z. Slawin, V. R. Seymour, S. E. Ashbrook and P. A. Wright,

Synthesis, Characterisation and Adsoprtion Properties of Microporous Scandium Carboxylates with Rigid and Flexible Frameworks,

Micro. Meso. Mater. 142, 322-333 (2011).

(77) M. R. Mitchell, S. W. Reader, K. E. Johnston, C. J. Pickard, K. R. Whittle and S. E. Ashbrook,

119Sn MAS NMR and First-Principles Calculations for the Investigation of Disorder in Pyrochlore Ceramics,

Phys. Chem. Chem. Phys. 13, 488-497 (2011).

(76) I. Bottero, B. Bonelli, S. E. Ashbrook, P. A. Wright, W. Zhou. M. Armandi and E. Garone,

Characterization of Hybrid Organic/Inorganic Nanotubes of the Imogolite Type,

Phys. Chem. Chem. Phys. 13, 744-750 (2011).

2010

(75) J. M. Griffin,  J. R. Yates, A. J. Berry, S. Wimperis and S. E. Ashbrook,

High-Resolution 19F MAS NMR Spectroscopy: Structural Disorder and Unusual J Couplings in a Fluorinated Silicate,

10. J.Am. Chem. Soc. 132, 15651-15660 (2010).
    

(74) M. Castro, V. R. Seymour, D. Carnevale, J. M. Griffin, S. E. Ashbrook, P. A. Wright, D. Apperley, J. E. Parker, S. Thompson, A. Fecant and N. Bats,

Molecular Modelling, Multinuclear NMR and Diffraction Studies in the Templated Synthesis and Characterisation of the Aluminophosphate Molecular Sieve STA-2,

J. Phys. Chem. C 114, 12698-12710 (2010).

(73) M. T. Wharmby, S. R. Miller, J. A. Groves, I. Marigold, S. E. Ashbrook and P. A. Wright,

Yttrium Bisphosphonate STA-13: A Racemic Phosphonate Metal Organic Framework with Permanent Porosity,

Dalton Trans. 39, 6389-6391 (2010).

(72) D. Carnevale, V. del Amo, D. Philp and S. E. Ashbrook,

Detecting Solid-State Reactivity in 10-hydroxy-10,9-Boroxophenanthrene using NMR Spectroscopy,

Tetrahedron 66, 6238-6250 (2010).

(71) K. E. Johnston, C. C. Tang, J. E. Parker, K. S. Knight, P. Lightfoot and S. E. Ashbrook,

The Polar Phase of NaNbO3: A Combined Study by Powder Diffraction, Solid-State NMR and First-Principles Calculations,

J. Am. Chem. Soc. 132, 8732-8746 (2010).

(70) P. S. Wheatley, P. K. Allan, S. J. Teat, S. E. Ashbrook and R. E. Morris,

Task Specific Ionic Liquids for the Ionothermal Synthesis of Pure Silica Zeolites,

Chem. Sci. 1, 483-487, (2010).

(69) D. R. Modeshia, R. I. Walton, M. R. Mitchell and S. E. Ashbrook,

Disordered Lithium Niobate Rock-Salt Materials Prepared by Hydrothermal Synthesis,

Dalton Trans. 39, 6031-6036 (2010).

(68) J. M. Griffin, A. J. Miller, A. J. Berry, S. Wimperis and S. E. Ashbrook,

Dynamics on the Microsecond Timescale in Hydrous Silicates Studied by Solid-State 2H NMR Spectroscopy,

Phys. Chem. Chem. Phys. 12, 2989-2998 (2010).

(67) Z. Han, A. L. Picone, A. M. Z. Slawin, V. R. Seymour, S. E. Ashbrook, W. Zhou, S. P. Thompson, J. E. Parker and P. A. Wright,

A Novel Large Pore Aluminophosphate Molecular Sieve STA-15 Prepared Using the Tetrapropylammonium Cation as a Structure Directing Agent,

Chem. Mater. 22, 338-346 (2010).

2009

(66) W. V. Maresch, M. D. Welch, M. Gottschalk, W. Ruthmann, M. Czank and S. E. Ashbrook,

Synthetic Amphiboles and Triple-Chain Silicates in the System Na2O-MgO-SiO2-H2O: Phase Characterization, Commpositional Relations and Excess H,

Mineral. Mag. 73(6), 957-996 (2009).

(65) H. Greer, P. S. Wheatley, S. E. Ashbrook, R. E. Morris and W. Zhou,

Early Stage Reversed Crystal Growth of Zeolite A and Phase Transformation to Sodalite,

J. Am. Chem. Soc. 131, 17986-17992 (2009).

(64) S. E. Ashbrook and S. Wimperis,

Spin-Locking of Half-Integer Quadrupolar Nuclei in Nuclear Magnetic Resonance of Solids: Second-Order Quadrupolar and Resonance Offset Effects ,

J. Chem. Phys. 131, 194509 (2009).

(63) S. W. Reader, M. R. Mitchell, K. E. Johnston, C. J. Pickard, K. R. Whittle and S. E. Ashbrook,

Cation Disorder in Pyrochlore Ceramics: 89Y MAS NMR and First-Principles Calculations,

J. Phys. Chem. C 113, 18874-18883 (2009).

(62) D. Carnevale, P. Wormald, B. Ameduri, R. Tayouo and S. E. Ashbrook,

Multinuclear Magnetic Resonance and DFT Studies of the Poly(chlorotrifluoroethylene-alt-ethyl vinyl ether) Copolymers,

Macromolecules 42, 5652-5659 (2009).

(61) S. E. Ashbrook,

Recent Advances in Solid-State NMR Spectroscopy of Quadrupolar Nuclei,

Phys. Chem. Chem. Phys. 11, 6892-6905 (2009).

(60) S. E. Ashbrook, J. McManus,  M. Thrippleton and S. Wimperis,

Second-Order Cross-term Interactions in High-Resolution MAS NMR of Quadrupolar Nuclei,

Prog. NMR Spectrosc. 55, 160-181 (2009). 

(59) S. E. Ashbrook, M. Cutajar, J. M. Griffin, Z. A. D. Lethbridge, R. I. Walton and S. Wimperis,

Transformation of AlPO-53 to JDF-2: Reversible Dehydration of a Templated Aluminophosphate Studied by MAS NMR and Diffraction,

J. Phys. Chem. C 113, 10780-10789 (2009). 

(58) N. S. Barrow, S. E. Ashbrook, S. P. Brown and D. Holland,

Developing 11B Solid-State NMR Methods to Characterise Medium Range Structure in Borates,

Phys. Chem. Glasses: Eur. J. Glass. Sci. Technol. B 50, 201-204 (2009).

(57) P. J. Byrne, J. E. Warren, R. E. Morris and S. E. Ashbrook,

Structure and NMR Assignment in AlPO-15: a Combined Study by Diffraction, MAS NMR and First-Principles Calculations,

Solid State Sciences 11, 1001 (2009).

(56) J. M. Griffin, S. Wimperis, A. J. Berry, C. J. Pickard and S. E. Ashbrook,

Solid-State 17O NMR Spectroscopy of Hydrous Magnesium Silicates: Evidence for Proton Dynamics,

J. Phys. Chem. C 113, 465-471 (2009).

(55) J. J. Williams, Z. A. D. Lethbridge, G. J. Clarkson, S. E. Ashbrook, K. E. Evans and R. I. Walton,

The Bulk Dissolution Method with Small Amines for the Synthesis of Large Crystals of the Siliceous Zeolites ZSM-22 and ZSM-48,

Micro. Meso. Mater. 119, 259-266 (2009).

(54) D. Modeshia, R. J. Darton, S. E. Ashbrook and R. I. Walton,

Control of Polymorphism in NaNbO3 by Hydrothermal Synthesis: Selective Preparation of Ilmenite over Perovskite Structure,

Chem. Commun. 68-70 (2009).

2008

(53) J. Cuny, S. Messaoudi, V. Alonzo, E. Furet, J. F. Halet, E. Le Fur, S. E. Ashbrook, C. J. Pickard, R. Gautier and L. Le Polles,

DFT Calculations of Quadrupolar Solid-State NMR Properties: Some Examples in Solid-State Inorganic Chemistry,

J. Comp. Chem. 13, 2279-2287 (2008).

(52) S. E. Ashbrook, M. Cutajar, C. J. Pickard, R. I. Walton and S. Wimperis,

Structure and NMR Assignment in Calcined and As-Synthesized Forms of AlPO-14: a Combined study by First-Principles Calculations and High-Resolution 27Al-31P MAS NMR Correlation,

Phys. Chem. Chem. Phys. 10, 5754-5764 (2008).

2007

(51) S. E. Ashbrook, A. J. Berry, A. Gregorovic, J. Readman and S. Wimperis,

17O and 29Si NMR Parameters of MgSiO3 Phases from High-Resolution Solid-State NMR Spectroscopy and First-Principles Calculations,

J. Am. Chem. Soc. 129, 13213-13224 (2007).

(50) C. S. Wright, R. I. Walton, D. Thompsett, J. Fisher and S. E. Ashbrook,

One-Step Hydrothermal Synthesis of Nanocrystalline Ceria-Zirconia Mixed Oxides,

Adv. Mater. 24, 4500-4504 (2007).

(49) K. R. Whittle, S. E. Ashbrook, G. R. Lumpkin, I. Farnan, R. I. Smith and S. A. T. Redfern,

The Effect of Caesium on Barium Hollandites Studied by Neutron Diffraction and Magic-Angle Spinning (MAS) Nuclear Magnetic Resonance,

J. Mater. Sci, 42, 9379-9391 (2007).

(48) S. E. Ashbrook, L. Le Polles, C. J. Pickard, A. J. Berry, S. Wimperis and I. Farnan,

First-Principles Calculations of Solid-State 17O and 29Si NMR Spectra of Mg2SiO4 Polymorphs,

Phys. Chem. Chem. Phys. 9, 1587-1598 (2007).

2006

(47) M. J. Thrippleton, T. Ball, S. Steuernagel, S. E. Ashbrook and S. Wimperis,

STARTMAS: a MAS-Based Method for Acquiring Isotropic NMR Spectra of Spin I = 3/2 Nuclei in Real Time

Chem. Phys. Lett. 431, 390-396 (2006).

(46) E. J. Harvey, S. E. Ashbrook, G. R. Lumpkin and S. A. T. Redfern,

Characterisation of the (Y1–xLax)2Ti2O7 System by Powder Diffraction and Nuclear Magnetic Resonance Methods,

J. Mater. Chem. 16, 4665-4674 (2006).

(45) M. D. Welch, A. R. Pawley, S. E. Ashbrook, H. E. Mason and B. L. Phillips,

Si Vacancies in the 10 Å Phase,

Am. Mineral. 91, 1707-1710 (2006).

(44) S. E. Ashbrook, L. Le Polles, R. Gautier, C. J. Pickard and R. I. Walton,

23Na Multiple-Quantum MAS NMR of the Perovskites NaNbO3 and NaTaO3,

Phys. Chem. Chem. Phys. 8, 3423-3431 (2006).

(43) S. Antonijevic, S. E. Ashbrook, S. Biedasek, R. I. Walton, S. Wimperis and H. Yang,

Dynamics on the Microsecond Timescale in Microporous Aluminophosphate AlPO-14 as evidenced by 27Al MQMAS and STMAS NMR Spectroscopy,

J. Am. Chem. Soc. 128, 8054-8062 (2006).

(42) J. F. Colin, T. Bataille, S. E. Ashbrook, N. Audebrand, L. Le Polles, J. Y. Pivan and E. Le Fur,

Na2[(VO)2(HPO4)2C2O4].2H2O: Crystal Structure and Determination from Combined Powder Diffraction and Solid State NMR,

Inorganic Chemistry, 45 6034-6040 (2006).

(41) S. E. Ashbrook, N. G. Dowell, I. Prokes and S. Wimperis,

Nuclear Overhauser Effect (NOE) Enhancement of 11B NMR Spectra of Borane Adducts in the Solid State,

J. Am. Chem. Soc. 128, 6782-6783 (2006).

(40) S. E. Ashbrook, K. R. Whittle, G. R. Lumpkin and I. Farnan,

89Y Magic-Angle Spinning NMR of Y2Ti2–xSnxO7 Pyrochlores,

J. Phys. Chem. B 110, 10358-10364 (2006).

(39) M. Cutajar, S. E. Ashbrook and S. Wimperis,

2H Double-Quantum MAS NMR Spectroscopy as a Probe of Dynamics on the Microsecond Timescale in Solids,

Chem. Phys. Lett. 423, 278-283 (2006).

(38) S. E. Ashbrook and M. E. Smith,

Solid State 17O NMR – An Introduction to the Background Principles and Applications to Inorganic Materials,

Chem. Soc. Rev. 35, 718-735 (2006).

(37) S. E. Ashbrook and M. J. Duer,

Structural Information from Quadrupolar Nuclei,

Concepts in Magn. Reson. 28A, 183-248 (2006).

(36) E. J. Harvey, S. E. Ashbrook, G. R. Lumpkin and S. A. T. Redfern,

Composition Driven Structural Phase Transitions in the (Y1–xLax)2Ti2O7 System,

Mat. Res. Symp. Proc. 932, 631-638 (2006).

(35) K. R. Whittle, G. R. Lumpkin and S. E. Ashbrook,

Neutron Diffraction and MAS NMR of Caesium Tungstate Defect Pyrochlores,

J. Solid State Chem. 179, 478-487 (2006).

2005

(34) S. E. Ashbrook and S. Wimperis,

Rotor-Synchronised Acquisition of Quadrupolar Satellite Transition NMR Spectra: Practical Aspects and Double-Quantum Filtration,

J. Magn. Reson. 177, 44-55 (2005).

(33) S. E. Ashbrook, A. J. Berry, W. O. Hibberson, S. Steuernagel and S. Wimperis,

High-Resolution 17O MAS NMR Spectroscopy of Forsterite (α-Mg2SiO4), Wadsleyite (β-Mg2SiO4) and Ringwoodite (γ-Mg2SiO4),

Am. Mineral. 90, 1861-1870 (2005).

(32) J. Roger, V. Babizhetsky, S. Cordier, J. Bauer, K. Hiebl, L. Le Polles, S. E. Ashbrook, J. F. Halet and R. Guerin,

Crystal Structures, Physical Properties and NMR Experiments on the Ternary Rare-Earth Metal Silicide Boride Compounds RE5Si~2B8 (RE = Y, Sm, Gd, Tb, Dy, Ho),

J. Solid State Chem. 178, 1854-1866 (2005).

(31) R. M. Orr, M. J. Duer and S. E. Ashbrook,

Correlating Fast and Slow Chemical Shift Spinning Sideband Patterns in Solid-State NMR,

J. Magn. Reson. 174, 301-309 (2005).

(30) S. E. Ashbrook, K. R. Whittle, L. Le Polles and I. Farnan,

Disorder and Dynamics in Pollucite from 133Cs and 27Al NMR,

J. Am. Ceram. Soc. 88, 1575-1583 (2005).

2004

(29) N. G. Dowell, S. E. Ashbrook and S. Wimperis,

Satellite-Transition MAS NMR of Low-γ Nuclei at Natural Abundance: Sensitivity, Practical Implementation and Application to 39K (I = 3/2) and 25Mg (I = 5/2),

J. Phys. Chem. B 108, 13292-13299 (2004).

(28) S. E. Ashbrook and I. Farnan,

Solid State 17O Nuclear Magnetic Resonance Spectroscopy Without Isotopic Enrichment: Direct Detection of Bridging Oxygen in Radiation Damaged Zircon,

Solid State Nucl. Magn. Reson. 26, 105-112 (2004).

(27) K. R. Whittle, G. R. Lumpkin and S. E. Ashbrook,

The Effect of Cs on the Structural Properties of Barium Titanate Hollandites,

Mat. Res. Symp. Proc. 824, 243-248 (2004).

(26) S. E. Ashbrook and S. Wimperis,

High-Resolution NMR of Quadrupolar Nuclei in Solids: The Satellite-Transition Magic Angle Spinning (STMAS) Experiment,

Prog. NMR Spectrosc. 45, 53-108 (2004).

(25) S. E. Ashbrook and S. Wimperis,

Spin-Locking of Quadrupolar Nuclei in Solids: Creation and Evolution of Coherences,

J. Chem. Phys. 120, 2719-2731 (2004).

2003

(24) S. E. Ashbrook, A. J. Berry, W. O. Hibberson, S. Steuernagel and S. Wimperis,

High-Resolution 17O NMR Spectroscopy of Wadsleyite (β-Mg2SiO4),

J. Am. Chem. Soc. 125, 11824-11825 (2003).

(23) K. R. Whittle, S. E. Ashbrook, S. A. T. Redfern, G. R. Lumpkin. J. P. Attfield, M. Dove and I. Farnan,

Structural Studies of Hollandite-Based Wasteforms,

Mat. Res. Symp. Proc. 807, 339-344 (2003).

(22) S. E. Ashbrook and S. Wimperis,

SCAM-STMAS: Satellite-Transition MAS NMR of Quadrupolar Nuclei with Self-Compensation for Magic-Angle Misset,

J. Magn. Reson. 162, 402-416 (2003).

(21) S. Wi, S. E. Ashbrook, S. Wimperis and L. Frydman,

Second-Order Quadrupolar-Shielding Effects in Magic-Angle Spinning Solid-State NMR,

J. Chem. Phys. 118, 3131-3140 (2003).

2002

(20) S. E. Ashbrook, S. Antonijevic. A. J. Berry and S. Wimperis,

Motional Broadneing: an Important Distinction Between Multiple-Quantum and Satellite-Transtion MAS NMR of Quadrupolar Nuclei,

Chem. Phys. Lett. 364, 634-642 (2002).

(19) N. G. Dowell, S. E. Ashbrook and S. Wimperis,

Relative Orientation of Quadrupole Tensors from High-Resolution NMR of Powdered Solids,

J. Phys. Chem. A 106, 9470-9478 (2002). (J. Phys. Chem. A 106, 12412-12412 (2002)).

(18) S. E. Ashbrook and S. Wimperis,

High-Resolution NMR of Quadrupolar Nuclei in Solids: Satellite-Transition MAS with Self-Compensation for Magic Angle Misset,

J. Am. Chem. Soc. 124, 11602-11603 (2002).

(17) S. E. Ashbrook and S. Wimperis,

Satellite-Transition MAS NMR of Spin I = 3/2, 5/2, 7/2 and 9/2 Nuclei: Sensitivity, Resolution and Practical Implementation,

J. Magn. Reson. 156, 269-281 (2002).

(16) S. Antonijevic, S. E. Ashbrook, R. I. Walton and S. Wimperis,

A Multiple-Quantum 23Na MAS NMR Study of Amorphous Sodium Gallium Zeolite Precursors,

J. Mater. Chem. 12, 1469-1474 (2002).

(15) S. E. Ashbrook, A. J. Berry and S. Wimperis,

17O Multiple-Quantum MAS NMR Study of Pyroxenes,

J. Phys. Chem. B 106, 773-778 (2002).

2001

(14) K. J. Pike, S. E. Ashbrook and S. Wimperis,

Two-Dimensional Satellite-Transition MAS NMR of Quadrupolar Nuclei: Shifted Echoes, HIgh-Spin Nuclei and Resolution,

Chem. Phys. Lett. 345, 400-408 (2001).

(13) N. G. Dowell, S. E. Ashbrook, J. McManus and S. Wimperis,

Relative Orientation of Quadrupole Tensors from Two-Dimensional Multiple-Quantum MAS NMR,

J. Am. Chem. Soc. 123, 8135-8136 (2001). (J. Am. Chem. Soc. 124, 1125-1125 (2002)).

(12) S. E. Ashbrook, K. J. D. MacKenzie and S. Wimperis,

27Al Multiple-quantum MAS NMR of Mechanically-Treated Bayerite (α-Al(OH)3) and Silica Mixtures,

Solid State Nucl. Magn. Reson. 20, 87-99 (2001).

(11) S. E. Ashbrook and S. Wimperis,

Novel Two-Dimensional Methods that Combine Single-Quantum Cross-Polarization and Multiple-Quantum MAS of Quadrupolar Nuclei,

Chem. Phys. Lett. 340, 500-508 (2001).

(10) S. E. Ashbrook, A. J. Berry and S. Wimperis,

17O Multiple-Quantum MAS NMR Study of High-Pressure Hydrous Magnesium Silicates,

J. Am. Chem. Soc. 123, 6360-6366 (2001).

(9) J. McManus, S. E. Ashbrook, K. J. D. MacKenzie and S. Wimperis,

27Al Multiple-Quantum MAS and 27Al(1H) CPMAS NMR Study of Amorphous Aluminosilicates,

J. Non-Cryst. Solids 282, 278-290 (2001).

2000

(8) S. E. Ashbrook and S. Wimperis,

Multiple-Quantum Cross-Polarization and Two-Dimensional MQMAS NMR of Quadrupolar Nuclei,

J. Magn. Reson. 147, 238-249 (2000).

(7) S. P. Brown, S. E. Ashbrook and S. Wimperis,

Reply to Comment on “27Al Multiple-Quantum Magic Angle Spinning NMR Study of the Thermal Transformation between the Microporous Aluminium Methylphosphonates AlMePO-β and AlMePO-α”,

J. Phys. Chem. B 104, 9767 (2000).

(6) K. J. Pike, R. M. Malde, S. E. Ashbrook, J. McManus and S. Wimperis,

Multiple-Quantum MAS NMR of Quadrupolar Nuclei. Do Five-, Seven- and Nine-Quantum Experiments Yield Higher Resolution than the Three-Quantum Experiment?,

Solid State Nucl. Magn. Reson. 16, 203-215 (2000).

(5) S. E. Ashbrook, J. McManus, K. J. D. MacKenzie and S. Wimperis,

Multiple-Quantum and Cross-Polarized 27Al MAS NMR of Mechanically-Treated Mixtures of Kaolinite and Gibbsite,

J. Phys. Chem. B 104, 6408-6416 (2000).

(4) S. E. Ashbrook and S. Wimperis,

Single- and Multiple-Quantum Cross-Polarization in NMR of Quadrupolar Nuclei in Static Samples,

Mol. Phys. 98, 1-26 (2000).

1999

(3) S. E. Ashbrook, A. J. Berry and S. Wimperis,

Three- and Five-Quantum 17O MAS NMR of Forsterite, Mg2SiO4,

Am. Mineral. 84, 1191-1194 (1999).

(2) S. P. Brown, S. E. Ashbrook and S. Wimperis,

27Al Multiple-Quantum Magic Angle Spinning NMR Study of the Thermal Transformation between the Microporous Aluminium Methylphosphonates AlMePO-β and AlMePO-α,

J. Phys. Chem. B 103, 812-817 (1999).

1998

(1) S. E. Ashbrook, S. P. Brown and S. Wimperis,

Multiple-Quantum Cross-Polarization in MAS NMR of Quadrupolar Nuclei,

Chem. Phys. Lett. 288, 509-517 (1998).