Publications for the Year 2002

Afzaal, M.; Aucott, S.M.; Crouch, D.; O'Brien, P.; Woollins, J.D.; Park, J.-H., Deposition of MSe (M = Cd, Zn) films by LP-MOCVD from novel single-source precursors M[(SePPh2)2N]2, Chem. Vap. Deposition, 2002, 8, 187-189.

Aitken, R.A.; Costello, S.J., Five-membered ring systems: with O & S (Se, Te) atoms in Progress in Heterocyclic Chemistry; G.W. Gribble and T.L. Gilchrist, Ed.; 2002, Vol. 14, 222-234.

Aitken, R.A.; Karodia, N.; Massil, T.; Young, R.J., Flash vacuum pyrolysis of stabilised phosphorus ylides. Part 17. Preparation of aliphatic amino acid derived g-alkoxycarbonyl-amino-b-oxo ylides and pyrolysis to give a,b-acetylenic g-amino acid and GABA analogues, J. Chem. Soc., Perkin Trans. 1, 2002, 533-541.

Aitken, R.A.; Hodgson, P.K.G.; Morrison, J.J.; Oyewale, A.O., Flash vacuum pyrolysis over magnesium. Part 1. Pyrolysis of benzylic, other aryl/alkyl and aliphatic halides, J. Chem. Soc., Perkin Trans. 1, 2002, 402-415.

Aitken, R.A.; Arumugam, S.; Mesher, S.T.E.; Riddell, F.G., Natural abundance 33S NMR spectroscopy. The first spectra of several major compound types, J. Chem. Soc., Perkin Trans. 2, 2002, 225-226.

Aitken, R.A.; Philp, E.F.; Riddell, F.G.; Smith, M.H., A synthetic and NMR conformational study of spiro cyclic quaternary ammonium salts, ARKIVOC, 2002, Issue in Honor of Dr Douglas Lloyd, 63-70.

Aitken, R.A.; Thomas, A.W., Flash vacuum pyrolysis of oxazolidine-2,4-diones, ARKIVOC, 2002, Issue in Honor of Dr Douglas Lloyd, 71-79.

Akopjan, A.V.; Serov, T.V.; Dolgikh, V.A.; Ardaschnikova, E.I.; Lightfoot, P., A new anion conductive bismuth-vanadium oxyfluoride, J. Mater. Chem., 2002, 12, 1490-1494.

* Allard, S.T.M.; Beis, K.; Giraud, M.F.; Hegeman, A.D.; Gross, J.W.; Wilmouth, R.C.; Whitfield, C.; Graninger, M.; Messner, P.; Allen, A.G.; Maskell, D.J.; Naismith, J.H., Toward a structural understanding of the dehydratase mechanism., Structure 10, 2002, 81-92.

Andreev, Y.; Bruce, P.G., Solution of flexible molecular structures by simulated annealing in Structure Determination from Powder Diffraction Data; W.I.F. David, K. Shankland, L.B. McCusker and Ch. Baerlocher, Ed.; Oxford University Press, 2002, Ch. 16, 286.

Appleby, T.; Woollins, J.D., Inorganic backbone phosphines, Coordination Chemistry Reviews, 2002, 235, 121-140.

Appleby, T.; Aucott, S.M.; Clarke, M.L.; Slawin, A.M.Z.; Woollins, J.D., Preparation and coordination chemistry of Ph2P(CH2)nNHPiPr 2 (n=2,3), Polyhedron, 2002, 21, 2639-2645.

Armstrong, A.R.; Paterson, A.J.; Robertson, A.D.; Bruce, P.G., Nonstoichiometric layered LixMnyO2 with a high capacity for lithium intercalation/deintercalation, Chem. Mater., 2002, 14, 710-719.

Asakawa, M.; Brancato, G.; Fanti, M.; Leigh, D.A.; Shimizu, T.; Slawin, A.M.Z.; Wong, J.K.Y.; Zerbetto, F.; Zhang, S., Switching "on" and "off" the expression of chirality in peptide rotaxanes, J. Am. Chem. Soc., 2002, 124, 2939-2950.

* Asuncion, M.; Blankenfeldt, W.; Barlow, J.N.; Gani, D.; Naismith, J.H., The structure of 3-methylaspartase from Clostridium tetanomorphum functions via the common enolase chemical step, J. Biol. Chem., 2002, 277, 8306-8311.

Aucott, S.M.; Slawin, A.M.Z.; Woollins, J.D., Synthesis and late transition metal complexes of the heterofunctional phosphane o-Ph2PNHC6H4P(S)Ph2, Eur. J. Inorg. Chem., 2002, 2408-2418.

Aucott, S.M.; Slawin, A.M.Z.; Woollins, J.D., The synthesis of [{n-Bu2Sn(S2N2)}2] and its use in the preparation of organometallic iridium sulfur nitrogen complexes, Can. J. Chem., 2002, 80, 1481-1487.

Baguley, P.A.; Jackson, L.V.; Walton, J.C., Preparation of 1-phenylcyclohexa-2,5-diene-1-carboxylates and their use in free-radical mediated syntheses, J. Chem. Soc., Perkin Trans. 1, 2002, 304-309.

Behm, M.; Irvine, J.T.S., Influence of structure and composition upon performance of tin phosphate based negative electrodes for lithium batteries, Electrochimica Acta, 2002, 47, 1727-1738.

Beier, P.; O'Hagan, D., Enantiomeric partitioning using fluorous biphase methodology for lipase-mediated (trans)esterifications, Chem. Comm., 2002, 1680-1681.

Bell, S.D.; Botting, C.H.; Wardleworth, B.N.; Jackson, S.P.; White, M.F., The interaction of alba, a conserved archaeal chromatin protein, with Sir2 and its regulation by acetylation, Science, 2002, 296, 148-151.

Bella, A.F.; Jackson, L.V.; Walton, J.C., A kinetic EPR study of the dissociation of 1-carbamoyl-1-methylcyclohexa-2,5-dienyl radicals: release of aminoacyl radicals and their cyclisation, J. Chem. Soc., Perkin Trans. 2, 2002, 1839-1843.

Bennett, R.N.; Mellon, F.A.; Botting, N.P.; Eagles, J.; Rosa, E.A.S.; Williamson, G., Identification of the major glucosinolate (4-mercaptobutyl glucosinolate) in leaves of Eruca sativa L. (salad rocket), Phytochemistry, 2002, 61, 25-30.

Bhattacharyya, P.; Slawin, A.M.Z.; Woollins, J.D., The reactivity of [PhP(Se)(u-Se)]2 and (PhP)3Se2 towards acetylenes and cyanamides: X-ray crystal structures of some P-Se-C and P-Se-C-N heterocycles, Chem. Eur. J., 2002, 8, 2705-2711.

* Blankenfeldt, W.; Kerr, I.D.; Giraud, M.F.; McMiken, H.J.; Leonard, G.A.; Whitfield, C.; Messner, P.; Graninger, M.; Naismith, J.H., Variation on a theme of SDR: dTDP-6-deoxy-L-lyxo-4-hexulose reductase (RmlD) shows a new Mg2+-dependent dimerisation mode in a well-known enzyme family, Structure 10, 2002, 773-786.

* Bloxham, J.; Moody, C.J.; Slawin, A.M.Z., Synthesis and solid state structures of N,N'-linked carbazoles and indoles, Tetrahedron, 2002, 58, 3709-3720.

* Boersma, B.J.; Patel, R.P.; Botting, N.P.; White, C.R.; Parks, D.; Barnes, S.; Darley-Usmar, V.M., Formation of novel bioactive metabolites from the reactions of pro-inflammatory oxidants with polyphenolics, Biofactors, 2002, 15, 79-81.

Bond, C.S.; White, M.F.; Hunter, W.N., Mechanistic implications for Escherichia coli cofactor-dependent phosphoglycerate mutase based on the high-resolution crystal structure of a vanadate complex, J. Mol. Biol., 2002, 316, 1071-1081.

Botting, C.H.; Davidson, N.E.; Griffiths, D.W.; Bennett, R.N.; Botting, N.P., Analysis of Intact Glucosinolates by MALDI-TOF Mass Spectrometry, J. Agric. Food Chem., 2002, 50, 983-988.

Bowes, K.F.; Ferguson, G.; Glidewell, C.; Lough, A.J.; Low, J.N.; Zakaria, C.M., N,N'-Dithiobisphthalimide–1,4-dioxan (1/0.6): a C2/c solvate with disordered solvent molecules localized in channels, Acta Cryst., 2002, C58, o347-o350.

Bowes, K.F.; Glidewell, C.; Low, J.N., Tetrameric triphenylsilanol, (Ph3SiOH)4, and the adduct (Ph3SiOH)2–dimethyl sulfoxide, both at 120 K, and the adduct (Ph3SiOH)4–1,4-dioxan at 150 K: interplay of O—H...O and C—H...p(arene) interactions, Acta Cryst., 2002, C58, o409-o415.

Bowes, K.F.; Ferguson, G.; Glidewell, C.; Lough, A.J., Self-assembled hydrogen-bonded bilayers in 1,4-diazabicyclo[2.2.2]-octane-N-(phosphonomethyl)iminodiacetic acid-water (1/1/1.5), Acta Cryst., 2002, C58, o467-o469.

Bowes, K.F.; Ferguson, G.; Glidewell, C.; Low, J.N.; Quesada, A., N,N'-Dithiobisphthalimide-nitro-benzene (2/1): a Pn solvate with localized solvent molecules ordered head-to-tail in channels, Acta Cryst., 2002, C58, o551-o554.

* Bruce, P.G.; Irvine, J.T.S., Intercalation compounds in Encyclopedia of Materials: Science and Technology; Elsevier, Oxford, 2002.

Bull, I.; Wheatley, P.S.; Lightfoot, P.; Morris, R.E.; Sastre, E.; Wright, P.A., Synthesis and crystal structure of the first scandium-containing open framework solid, Chem. Commun., 2002, 1180-1181.

Butler, A.R.; Megson, I.L., Non-heme iron nitrosyls in biology, Chem. Rev., 2002, 102, 1155-1165.

Butler, A.R.; Brown, E.H., Condensation of 2-hydroxy-2'-aminoacetophenone to form a dihydropyrazine, ARKIVOC, 2002, Issue in Honor of Dr Douglas Lloyd, 166-171.

Byabartta, P.; Jasimuddin, S.; Ghosh, B.K.; Sinha, C.; Slawin, A.M.Z.; Woollins, J.D., Nitro-ruthenium(II)-arylazoimidazoles: synthesis, spectra, crystal structure and electrochemistry of dinitro-bis{1-alkyl-2-(arylazo)imidazole}ruthenium(II). Nitro-nitroso derivatives and reactivity of the electrophilic {Ru-NO}6 system, New J. Chem., 2002, 26, 1415-1424.

Canales-Vázquez, J.; Zhou, W.; Irvine, J.T.S., Characterisation of novel anodes for solid oxide fuel cells based on oxygen-excess perovskite related structures, Ionics, 2002, 8, 252-255.

* Cassidy, A.; Faughnan, M.S.; Avades, T.; Zimmer-Nechemias, L.; Wolfe, B.E.; Brashear, W.T.; Botting, N.P.; Oldfield, M.F.; Setchell, K.D.R.; Desai, P., Pharmacokinetic behaviour of [C-13]daidzein and [C-13]genistein in humans, J. Nutr., 2002, 132, 594.

Chen, Q.; Zhou, W.; Du, G.; Peng, L.-M., Trititanate nanotubes made via a single alkali treatment, Adv. Mater., 2002, 14, 1208-1211.

Chen, Q.; Rada, T.; McDowall, A.; Richardson, N.V., Epitaxial growth of a crystalline organic semiconductor: Perylene/Cu{110}, Chem. Mater., 2002, 14, 743-749.

Chen, Q.; Frankel, D.J.; Richardson, N.V., Chemisorption induced chirality: glycine on Cu{110}, Surface Science, 2002, 497, 37-46.

* Chen, Q.; Frankel, D.J.; Richardson, N.V., Dehydrogenation induced phase transitions of p-aminobenzoic acid on Cu(110), J. Chem. Phys., 2002, 116, 455-459.

* Chen, Q.; Frankel, D.J.; Richardson, N.V., Self-assembly of adenine on Cu(110) surfaces, Langmuir, 2002, 18, 3219-3225.

Cheshire, P.; Slawin, A.M.Z.; Woollins, J.D., First example of a Rh-N-C-O-P heterocycle - a rare example of a five membered true heterocycle, Inorganic Chemistry Communications, 2002, 5, 803-804.

Clarke, D.B.; Lloyd, A.S.; Botting, N.P.; Oldfield, M.F.; Needs, P.W.; Wiseman, H., Measurement of intact sulfate and glucuronide phytoestrogen conjugates in human urine using isotope dilution liquid chromatography-tandem mass spectrometry with [13C3]isoflavone internal standards, Analytical Biochemistry, 2002, 309, 158-172.

Clarke, M.L.; Cole-Hamilton, D.J.; Foster, D.F.; Slawin, A.M.Z.; Woollins, J.D., Co-ordination chemistry and metal catalysed carbonylation reactions using 8-(diphenylphosphino)methylaminoquinoline: a ligand that displays monodentate, bidentate and tridentate co-ordination modes, J. Chem. Soc., Dalton Trans., 2002, 1618-1624.

Clarke, M.L.; Holliday, G.L.; Slawin, A.M.Z.; Woollins, J.D., Highly electron rich alkyl- and dialkyl-N-pyrrolidinyl phosphines: an evaluation of their electronic and structural properties, J. Chem. Soc., Dalton Trans., 2002, 1093-1103.

Cole-Hamilton, D.J.; Sellin, M.; Webb, P., Catalysis in an ionic fluid, supercritical fluid two phase system, in WO 02/02218 A1; International, 2002; pp.

Connor, P.A.; Irvine, J.T.S., Combined X-ray study of lithium (tin) cobalt oxide matrix negative electrodes for Li-ion batteries, Electrochimica Acta, 2002, 47, 2885-2892.

Connor, P.A.; Belliard, F.; Behm, M.; Tovar, L.G.; Irvine, J.T.S., How amorphous are the tin alloys in Li-inserted tin oxides?, Ionics, 2002, 8, 172-176.

Danks, M.J.; Jervis, H.B.; Nowotny, M.; Zhou, W.; Maschmeyer, T.A.; Bruce, D.W., High-activity heterogeneous catalysts prepared in one step from the mesophases of metallosurfactants, Catalysis Letters, 2002, 82, 95-98.

Dicke, C.; Morstein, M.; Hähner, G., Surface inorganic chemistry: the reaction of hydroxyl-terminated thiols on gold with a zirconium coordination compound, Langmuir, 2002, 18, 336-344.

Dicke, C.; Hähner, G., Interaction between a hydrophobic probe and tri(ethylene glycol)-containing self-assembled monolayers on gold studied with force spectroscopy in aqueous electrolyte solution, J. Phys. Chem. B, 2002, 106, 4450-4456.

Dicke, C.; Hähner, G., pH-Dependent force spectroscopy of tri(ethylene glycol)- and methyl-terminated self-assembled monolayers adsorbed on gold, J. Am. Chem. Soc., 2002, 124, 12619-12625.

* Dransfield, P.J.; Gore, P.M.; Shipman, M.; Slawin, A.M.Z., Divergent approach to imino sugar C-glycosides using imino glycols; application to the stereocontrolled synthesis of (+)-deoxoprosophyline, Chem. Comm., 2002, 150-151.

Eastham, G.R.; Tooze, R.P.; Kilner, M.; Foster, D.F.; Cole-Hamilton, D.J., Deuterium labelling evidence for a hydride mechanism in the formation of methyl propanoate from carbon monoxide ethene and methanol catalysed by a palladium complex, J. Chem. Soc., Dalton Trans., 2002, 1613-1617.

Edgar, M.; Carter, V.J.; Tunstall, D.P.; Grewal, P.; Favre-Nicolin, V.; Cox, P.A.; Lightfoot, P.; Wright, P.A., Structure solution of a novel aluminium methylphosphonate using a new simulated annealing program and powder X-ray diffraction data, Chem. Commun., 2002, 808-809.

Edgar, M.; Carter, V.J.; Grewal, P.; Sawers, L.-J.; Sastre, E.; Tunstall, D.P.; Cox, P.A.; Lightfoot, P.; Wright, P.A., Structure elucidation of a novel aluminum methylphosphonate, Al3(CH3PO3)2.O.(OH) 3, through a combination of X-ray powder diffraction, solid-state NMR spectroscopy, and computational energy minimization, Chem. Mater., 2002, 14, 3432-3439.

Evans, I.R.; Tao, S.; Irvine, J.T.S.; Howard, J.A.K., Synthesis, crystal structure, and oxide ion conductivity in Bi4.6Ca1.1VO10.5, Chem. Mater., 2002, 14, 3700-3704.

Farrell, D.M.M.; Ferguson, G.; Lough, A.J.; Glidewell, C., Chiral versus racemic building blocks in supramolecular chemistry: malate salts of organic diamines, Acta Cryst., 2002, B58, 530-544.

Farrell, D.M.M.; Ferguson, G.; Lough, A.J.; Glidewell, C., A structural hierarchy in the hydrogen-bonded adduct N,N'-dimethylpiperazine–tartaric acid–water(1/2/2): an N-component N-dimensional structure (N = 3) with substructures having N = 1 and 2, Acta Cryst., 2002, C58, o6-o8.

Farrell, D.M.M.; Ferguson, G.; Lough, A.J.; Glidewell, C., Chiral versus racemic building blocks in supramolecular chemistry: tartrate salts of organic diamines, Acta Cryst., 2002, B58, 272-288.

Farrell, D.M.M.; Glidewell, C.; Low, J.N.; Skakle, J.M.S.; Zakaria, C.M., Polymorphs and pseudopolymorphs of N,N'-dithiobisphthalimide, Acta Cryst., 2002, B58, 289-299.

Foster, D.F.; Adams, D.J.; Gudmunsen, D.; Stuart, A.M.; Hope, E.G.; Cole-Hamilton, D.J., Hydroformylation in fluorous solvents, Chem. Commun., 2002, 722-723.

Foster, D.F.; Gudmunsen, D.; Adams, D.J.; Stuart, A.M.; Hope, E.G.; Cole-Hamilton, D.J.; Schwarz, G.P.; Pogorzelec, P., Hydroformylation in perfluorinated solvents; improved selectivity, catalyst retention and product separation, Tetrahedron, 2002, 58, 3901-3910.

* Frankel, D.J.; Chen, Q.; Richardson, N.V., Adsorption of a-pyridone on Cu(110), J. Chem. Phys., 2002, 116, 8988-8993.

Frey, S.; Rong, H.-T.; Heister, K.; Yang, Y.-J.; Buck, M.; Zharnikov, M., Response of biphenyl-substituted alkanethiol self-assembled monolayers to electron irradiation: damage suppression and odd-even effects, Langmuir, 2002, 18, 3142-3150.

Galbraith, S.C.; Robson, C.R.; Richens, D.T., Variable-pressure kinetic study of bromide complexation on aquarhodium(III), J. Chem. Soc., Dalton Trans., 2002, 4335-4338.

Garcia-Bennett, A.E.; Williamson, S.; Wright, P.A.; Shannon, I.J., Control of structure, pore size and morphology of three-dimensionally ordered mesoporous silicas prepared using the dicationic surfactant [CH3(CH2)15N(CH3) 2(CH2)3N(CH3)3]Br 2, J. Mater. Chem., 2002, 12, 3533-3540.

Garden, S.J.; da Cunha, F.R.; Wardell, J.L.; Skakle, J.M.S.; Low, J.N.; Glidewell, C., 2,6-Diiodo-4-nitrophenol, 2,6-diiodo-4-nitrophenyl acetate and 2,6-diiodo-4-nitroanisole: interplay of hydrogen bonds, iodo-nitro interactions and aromatic p-p-stacking interactions to give supramolecular structures in one, two and three dimensions, Acta Cryst., 2002, C58, o463-o466.

Garden, S.J.; Fontes, S.P.; Wardell, J.L.; Skakle, J.M.S.; Low, J.N.; Glidewell, C., Interplay of hydrogen bonds, iodo...nitro interactions and aromatic p...p stacking interactions in iodo-nitroanilines, Acta Cryst., 2002, B58, 701-709.

Gibson, J.F.; Mackie, R.K.; Marshall, D.R., A tribute to Douglas Lloyd, ARKIVOC, 2002, Issue in Honor of Dr Douglas Lloyd, 1-18.

Giménez-Saiz, C.; Slawin, A.M.Z.; Woollins, J.D., Original packing and unusual molecular conformation of the bis(ethylenedithio tetrathiafulvalene (ET) donors induced by cation-anion interactions in the radical salt ET5[B10I10](CH2Cl2)0.8, CrystEngComm, 2002, 15.

Glidewell, C.; Low, J.N.; Skakle, J.M.S.; Wardell, J.L., Hydrogen-bonded molecular ladders in S-(4-nitrophenyl)thioglycolic acid, Acta Cryst., 2002, C58, o201-o203.

Glidewell, C.; Low, J.N.; Bomfim, J.A.S.; Filgueiras, C.A.L.; Wardell, J.L., catena-Poly[[triphenyltin(IV)]-m-hydroxo- K2O:O] at 120 K, Acta Cryst., 2002, C58, m199-m201.

Glidewell, C.; Low, J.N.; Cobo, J.; Nogueras, M.; Sánchez, A.; Rengifo, E.; Abonia, R., 5-[N-(1H-Benzotriazol-1-ylmethyl)-amino]-3-tert-butyl-1-phenylpyrazole: sheets built from N—H...N, C—H...N and C—H...p(pyrazole) interactions, Acta Cryst., 2002, C58, o314-o317.

Glidewell, C.; Low, J.N.; Mascarós, P.A.; Martos, R.C.; Valero, M.D.G., catena-Poly[[[{N-(6-amino-3,4-dihydro-3-methyl-5-nitroso-4-oxopyrimidin-2-yl)glycinato- O}pentaaquastrontium]-u-N-(6-amino-3,4-dihydro-3-methyl-5-nitroso-4-oxopyrimidin-2-yl)glycinato- O:O'] monohydrate]: coordination polymer chains linked by hydrogen bonds into a three-dimensional framework, Acta Cryst., 2002, C58, m61-m64.

Glidewell, C.; Low, J.N.; McWilliam, S.A.; Skakle, J.M.S.; Wardell, J.L., Hydrogen bonding in C-substituted nitroanilines: molecular ladders in 2-trifluoromethyl-4-nitroaniline and sheets of R44(12) and R44(32) rings in 3-trifluoromethyl-4-nitroaniline, Acta Cryst., 2002, C58, o97-o99.

Glidewell, C.; Low, J.N.; McWilliam, S.A.; Skakle, J.M.S.; Wardell, J.L., Hydrogen bonding in C-substituted nitroanilines: sheets built from alternating R22(12) and R66(36) rings in 2-bromo-6-cyano-4-nitroaniline, Acta Cryst., 2002, C58, o100-o102.

Glidewell, C.; Low, J.N.; Skakle, J.M.S.; Wardell, S.M.S.V.; Wardell, J.L., 2-Iodo-N-(3-nitrobenzyl)aniline and 3-iodo-N-(3-nitrobenzyl)aniline exhibit entirely different patterns of supramolecular aggregation, Acta Cryst., 2002, C58, o487-o490.

Glidewell, C.; Howie, R.A.; Low, J.N.; Skakle, J.M.S.; Wardell, S.M.S.V.; Wardell, J.L., Nine isomeric nitrobenzylidene-iodoanilines: interplay of C—H...O hydrogen bonds, iodo...nitro interactions and aromatic p...p stacking interactions, Acta Cryst., 2002, B58, 864-876.

Glidewell, C.; Low, J.N.; Marchal, A.; Melguizo, M.; Quesada, A., 2-Amino-4,6-dimethoxy-5-nitroso-pyrimidine-water (4/3): seven independent molecular components are linked into a three-dimensional framework by six three-centre and eight two-centre hydrogen bonds, Acta Cryst., 2002, C58, o655-o657.

Glidewell, C., Review of book by Jack Barrett entitled "Structure and Bonding", Chemistry & Industry, 2002, 1st July, 25.

Glidewell, C.; Low, J.N.; Skakle, J.M.S.; Wardell, J.L., 2-Nitrophenyl 4-nitrophenyl disulfide, Acta Cryst., 2002, C58, o485-o486.

Gomez, S.; Peters, J.A.; van der Waal, J.C.; Zhou, W.; Maschmeyer, T., Preparation of benzylamine by highly selective reductive amination of benzaldehyde over Ru on an acidic activated carbon support as the catalyst, Catalysis Letters, 2002, 84, 1-5.

Grewal, P.; Wright, P.A.; Edgar, M.; Gale, J.D.; Cox, P.A., Modelling the structure and properties of aluminophosphonates, Mat. Res. Soc. Symp. Proc., San Francisco, 2002, 726, Q2.5.

* Hayes, J.F.; Shipman, M.; Slawin, A.M.Z.; Twin, H., Multi-component reactions of 2-isopropylidene-aziridines: application to the synthesis of enantiopure neopentylamines, Heterocycles, 2002, 58, 243-250.

* Hähner, G., Dyes on mica mineral surfaces in Encyclopedia of Surface and Colloid Science; A. Hubbard, Ed.; M. Dekker Publishing, 2002.

Hervoches, C.H.; Snedden, A.; Riggs, R.; Kilcoyne, S.H.; Manuel, P.; Lightfoot, P., Structural behavior of the four-layer aurivillius-phase ferroelectrics SrBi4Ti4O15 and Bi5Ti3FeO15, J. Solid State Chem., 2002, 164, 280-291.

* Hofer, W.A.; Fisher, A.J.; Bitzer, T.; Rada, T.; Richardson, N.V., Tuning in on single molecular states: adsorption sites and STM images of maleic anhydride on Si(100), Chem. Phys. Letters, 2002, 355, 347-354.

Hunter, H.M.A.; Garcia-Bennett, A.E.; Shannon, I.J.; Zhou, W.; Wright, P.A., Particle morphology and microstructure in the mesoporous silicate SBA-2, J. Mater. Chem., 2002, 12, 20-23.

* Hunter, A.D.; Woollins, J.D., Discovery based experiments in organometallic chemistry, Abst. Pap. Am. Chem. Soc., 2002, 223, 1.

Irvine, J.T.S.; Corcoran, D.J.D.; Canales-Vazquez, J., Structural studies of the distorted perovskite proton conductors Sr3Ca1+xNb2–xO9–d, Solid State Ionics, 2002, 152-153, 749-757.

Irvine, J.T.S.; Corcoran, D.J.D.; Lashtabeg, A.; Walton, J.C., Incorporation of molecular species into the vacancies of perovskite oxides, Solid State Ionics, 2002, 154-155, 447-453.

Jain, S.L.; Crayston, J.A.; Richens, D.T.; Woollins, J.D., Spectroelectrochemistry of copper(II) complexes with deprotonated tetradentate pyridine-2-carboxamide ligands: EC reaction of the electrogenerated Cu(III) species, Inorg. Chem. Comm., 2002, 5, 853-855.

Jones, T.E.; Baddeley, C.J., A RAIRS, STM and TPD study of the Ni{111}/R,R-tartaric acid system: Modelling the chiral modification of Ni nanoparticles, Surface Science, 2002, 513, 453-467.

Jones, F.G.E.; Irvine, J.T.S., Preparation of thin films using the tape-casting process for use in the solid oxide fuel cell, Ionics, 2002, 8, 339-343.

Jones, T.E.; Baddeley, C.J., Direct STM evidence of a surface interaction between chiral modifier and pro-chiral reagent: Methylacetoacetate on R,R-tartaric acid modified Ni{111}, Surface Science, 2002, 519, 237-249.

Jones, T.E.; Noakes, T.C.Q.; Bailey, P.; Baddeley, C.J., Structural and compositional analysis of two ordered near-surface alloys produced by adsorption and thermal decomposition of Mo(CO)6 on Ni{111}, Surface Science, 2002, 523, 12-20.

Kaltenpoth, G.; Völkel, B.; Nottbohm, C.T.; Gölzhäuser, A.; Buck, M., Electrode modification by electron-induced patterning of self-assembled monolayers, J. Vac. Sci. Technol. B, 2002, 20, 2734-2738.

Kelly, C.J.; Skakle, J.M.S.; Wardell, J.L.; Wardell, S.M.S.V.; Low, J.N.; Glidewell, C., Iodo-nitroarenesulfonamides: interplay of hard and soft hydrogen bonds, I...O interactions and aromatic p...p stacking interactions, Acta Cryst., 2002, B58, 94-108.

Kennedy, R.D.; Lloyd, D.; McNab, H., Annulenes, 1980-2000, J. Chem. Soc., Perkin Trans. 1, 2002, 1601-1621.

Kusainova, A.M.; Zhou, W.; Irvine, J.T.S.; Lightfoot, P., Layered intergrowth phases Bi4MO8X (X=Cl, M=Ta, and X=Br, M=Ta or Nb): Structural and electrohphysical characterization, J. Solid State Chem., 2002, 166, 148-157.

Kusainova, A.M.; Stefanovich, S.Y.; Irvine, J.T.S.; Lightfoot, P., Structure-property correlations in the new ferroelectric Bi5PbTi3O14Cl and related layered oxyhalide intergrowth phases, J. Mater. Chem., 2002, 12, 3413-3418.

Kvaratskhelia, M.; Wardleworth, B.N.; Bond, C.S.; Fogg, J.M.; Lilley, D.M.J.; White, M.F., Holliday junction resolution is modulated by archaeal chromatin components in vitro, J. Biological Chem., 2002, 277, 2992-2996.

Laurent, P.; Miyaji, H.; Collinson, S.R.; Prokes, I.; Moody, C.J.; Tucker, J.H.R.; Slawin, A.M.Z., Asymmetric synthesis of chiral a-ferrocenylalkylamines and their use in the preparation of chiral redox-active receptors, Org. Lett., 2002, 4, 4037-4040.

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Low, J.N.; Quesada, A.; Marchal, A.; Nogueras, M.; Sánchez, A.; Glidewell, C., 4-Amino-6-benzyloxy-2-(methyl-sulfanyl)-5-nitrosopyrimidine: hydrogen-bonded dimers linked into p-stacked chains, Acta Cryst., 2002, C58, o284-o286.

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* Manos, M.J.; Woollins, J.D.; Keramidas, A.D.; Slawin, A.M.Z.; Kabanos, T.A., The first poloxomolybdenum(V)-sulfite compounds. Structural and physical studies of (NH4)20[Mo2VO4) 6(u2-SO3)12(u 3-SO3)4].4H2O 1, (NH4)15{Na[Mo2VO4) 3(u2-O)3(u2-SO 3)4(u;6-SO3)]2}.5H 2O 2 and (NH4)8[(Mo2VO4)(SO 3)4(u2-SO3)].2H 2O 3, Angewandte Chemie Int. Ed. Engl., 2002, 41, 2801-2805.

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McCarroll, A.J.; Walton, J.C., On the preparation of cyclopentadienes by a novel homolytic annulation of but-3-en-1-ones with alkynes mediated by samarium diiodide, ARKIVOC, 2002, Issue in Honor of Dr Douglas Lloyd, 55-62.

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McConnell, A.; Lightfoot, P.; Richens, D.T., Crystal structure and kinetics of the acid-catalysed decomposition of (N,N'-bis(2-pyridylmethylene)-1,3-diamino-2,2-dicarboxyethylpropane)copper(II)perchlorate, Inorganica Chimica Acta, 2002, 331, 143-150.

* Merkel, A.B.; Temple, G.; Beis, K.; Bukart, M.; Walsh, C.T.; Naismith, J.H., The purification, crystallisation and preliminary structural characterisation of an epimerase (EvaD), the fourth enzyme in the vancosamine biosynthetic pathway, Acta Cryst., 2002, 58, 1226-1228.

Morton, C.J.H.; Gilmour, R.; Smith, D.M.; Lightfoot, P.; Slawin, A.M.Z.; MacLean, E.J., Synthetic studies related to diketopyrrolopyrrole (DPP) pigments. Part 1: The search for alkenyl-DPPs. Unsaturated nitriles in standard DPP syntheses: a novel cyclopenta[c]pyrrolone chromophore, Tetrahedron, 2002, 58, 5547-5565.

Muirhead, K.M.; Botting, N.P., The synthesis of 5-fluorokynurenine and 6-fluorokynurenic acid as metabolic probes, ARKIVOC, 2002, 2, 37-45.

Nanni, D.; Pareschi, P.; Walton, J.C., An electron paramagnetic resonance study of intermediates generated from aromatic aldimines, J. Chem. Soc., Perkin Trans. 2, 2002, 1098-1104.

Nicoletti, M.; O'Hagan, D.; Slawin, A.M.Z., The asymmetric Bischler-Napieralski reaction: preparation of 1,3,4-trisubstituted 1,2,3,4-tetrahydroisoquinolines, J. Chem. Soc., Perkin Trans. 1, 2002, 116-121.

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Patterson, S.; O'Hagan, D., Biosynthetic studies on the tropane alkaloid hyoscyamine in Datura stramonium; hyoscyamine is stable to in vivo oxidation and is not derived from littorine via a vicinal interchange process, Phytochemistry, 2002, 61, 323-329.

Platas-Iglesias, C.; Vander Elst, L.; Zhou, W.; Muller, R.N.; Geraldes, C.F.G.C.; Maschmeyer, T.; Peters, J.A., Zeolite GdNaY Nanoparticles with very high relaxivity for application as contrast agents in Magnetic Resonance Imaging, Chem. Eur. J., 2002, 8, 5121-5131.

* Plater, M.J.; Foreman, M.R.S.J.; De Silva, B.M.; Shakle, J.M.S.; Slawin, A.M.Z., Synthesis and crystal structure of [Cu2(NO3)4]L2(bipy) 2(H2O)3]H2O (L = N,N'-bis(4-pyridylmethyl)isophthalamide, J. Chem. Cryst., 2002, 32, 5-10.

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Reid, D.H.; (the late) Dingwall, J.G., Preparation of 4-thia-10b-azaindeno[2,1,7-lma]fluorenes, ARKIVOC, 2002, Issue in Honor of Dr Douglas Lloyd, 140-142.

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Riddell, F.G., Intramolecular motions in solid organic compounds in Encyclopedia of Nuclear Magnetic Resonance; D.M. Grant and R.K. Harris, Ed.; John Wiley & Sons, Ltd, Chichester, 2002, Vol. 9, 570-578.

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Rodriguez i Zubiri, M.; Slawin, A.M.Z.; Wainwright, M.; Woollins, J.D., The preparation and coordination chemistry of phosphorus(III) derivatives of piperazine and homopiperazine, Polyhedron, 2002, 21, 1729-1736.

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Ropartz, L.; Morris, R.E.; Foster, D.F.; Cole-Hamilton, D.J., Phosphine-containing carbosilane dendrimers based on polyhedral silsesquioxane cores as ligands for hydroformylation reaction of oct-1-ene, J. Mol. Catal. A: Chemical, 2002, 182-183, 99-105.

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Scanlan, E.M.; Walton, J.C., Preparation of oxime oxalate amides and their use in free-radical mediated syntheses of lactams, Chem. Commun., 2002, 2086-2087.

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Shan, Z.; Zhou, W.; Jansen, J.C.; Yeh, C.Y.; Koegler, J.H.; Maschmeyer, T., Incorporation of nano-sized zeolites into a mesoporous matrix, TUD-1, Studies in Surface Science and Catalysis, 2002, 141, 635-640.

Shen, S.; Li, Y.; Zhang, Z.; Fan, J.; Tu, B.; Zhou, W.; Zhao, D., A novel ordered cubic mesoporous silica templated with tri-head group quaternary ammonium surfactant, Chem. Commun., 2002, 2212-2213.

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* Taher, A.; Eishenseher, S.; Slawin, A.M.Z.; Weaver, G.W., Synthesis of 2-aryl-2H,4H-imidazo[4,5-d][1,2,3]triazoles from triethyl N-(1-ethyl-2-methyl-4-nitro-1H-imidazol-5-yl) phosphorimidate by reaction with aryl isocyanates, J. C. S. Perkin 1, 2002, 1968-1972.

Tao, S.; Irvine, J.T.S., Study on the structural and electrical properties of the double perovskite oxide SrMn0.5Nb0.5O3–d, J. Mater. Chem., 2002, 12, 2356-2360.

Tao, S.; Irvine, J.T.S., Optimization of mixed conducting properties of Y2O3-ZrO2-TiO2 and Sc2O3-Y2O3-ZrO2-TiO 2 solid solutions as potential SOFC anode materials, J. Solid State Chem., 2002, 165, 12-18.

Tao, S.; Irvine, J.T.S., Structure and properties of nonstoichiometric mixed perovskites A3B'1+xB"2–xO9–d, Solid State Ionics, 2002, 154-155, 659-667.

Tasiopoulos, A.J.; Tolis, E.J.; Tsangaris, J.M.; Evangelou, A.; Woollins, J.D.; Slawin, A.M.Z.; Pessoa, J.C.; Coreia, I.; Kabanos, T.A., Model investigations for vanadium-protein interactions: vanadium(III) compounds with dipeptides and their oxovanadium(IV) analogues, J. Biol. Inorg. Chem., 2002, 7, 363-374.

Tavasli, M.; Courtieu, J.; Goss, R.J.M.; Meddour, A.; O'Hagan, D., Extreme enantiomeric discrimination of fluoroalkanes using deuterium NMR in chiral liquid crystalline media, Chem. Comm., 2002, 844-845.

Tavasli, M.; O'Hagan, D.; Pearson, C.; Petty, M., The fluorine gauche effect. Langmuir isotherms report the relative conformational stability of (±)-erythro- and (±)-threo-9,10-difluorostearic acids, Chem. Comm., 2002, 1226-1227.

Tremayne, M.; Seaton, C.C.; Glidewell, C., Structures of three substituted arenesulfonamides from X-ray powder diffraction data using the differential evolution technique, Acta Cryst., 2002, B58, 823-834.

Villaescusa, L.A.; Lightfoot, P.; Morris, R.E., Synthesis and structure of fluoride-containing GeO2 analogues of zeolite double four-ring building units, Chem. Commun., 2002, 2220-2221.

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Wheatley, P.S.; Love, C.J.; Morrison, J.J.; Shannon, I.J.; Morris, R.E., Synthesis of two new aluminophosphate based layered materials using Tet-A as a structure-directing agent, J. Mater. Chem., 2002, 12, 477-482.

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Yuan, Z.-Y.; Zhou, W.; Su, B.-L., Hierarchical interlinked structure of titanium oxide nanofibers, Chem. Commun., 2002, 1202-1203.

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Zakaria, C.M.; Ferguson, G.; Lough, A.J.; Glidewell, C., [Ni(cyclam)(OCOR)2], a finite molecular complex: hydrogen-bonded supramolecular aggregation in one, two and three dimensions, and coordination polymers in one and two dimensions, Acta Cryst., 2002, B58, 78-93.

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Zhang, Q.; Aucott, S.M.; Slawin, A.M.Z.; Woollins, J.D., Synthesis and coordination chemistry of the new unsymmetrical ligand Ph2PCH2NHC6H4PPh2, Eur. J. Inorg. Chem., 2002, 1635-1646.

Zhou, W.; Garcia-Bennett, A.E.; Hunter, H.M.A.; Wright, P.A., Electron microscopic investigation of mesoporous SBA-2, Studies in Surface Science and Catalysis, 2002, 141, 379-386.

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* No reprints available.

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